China Factory Direct
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| CAS number | 17318-03-5 |
| Product name | 3-FLUOROPHENYLMAGNESIUM BROMIDE |
| Stock | Stock readily available; annual supply capacity exceeding 1,000 tons. |
| Grade | Agricultural GradeMaterial GradeSpecialty GradeReagent GradeIndustrial Grade |
| Packaging | 25L/drum200L/drum1000L/IBC |
| Sample | Test Samples Available (Click to Request Samples) |
| COA | View COA |
| Price | Get Quote |
| Supply Type | Bulk / Contract manufacturing / OEM |
| Shipping | FCL / LCL available |
| Payment Terms | Support FOB \ CIF \ EXW quotations, and accept Letter of Credit (L/C). |
| Manufacturer | Greenrock Chemical(China Factory) |
Based on current marketvolatility and material availability.
17+ years in chemical exports.Fully compliant, reliable supply.Your B2B partner in bulk chemical procurement.
| Industry | Application | Process |
|---|---|---|
| Pharmaceuticals | As an organic synthesis intermediate for preparing fluorinated drug molecules (e.g., antidepressants, anti-inflammatory agents) | Grignard reagent reaction—forms C–C bonds via reaction with electrophilic reagents such as aldehydes, ketones, and esters |
| Agrochemicals | Synthesis of fluorinated active ingredients (e.g., herbicides, fungicides) | Introduces the 3-fluorophenyl group via Grignard reaction, followed by further derivatization |
| Materials Science | Preparation of fluorinated liquid crystal materials or polymer monomers | Reacts with silanes, alkyl halides, and other reagents to generate functional monomers |
| Fine Chemicals | Synthesis of fluorinated fine chemicals, including fluorescent dyes and fragrances | Acts as a nucleophile in coupling and substitution reactions |
| Research | Structural modification and mechanistic studies of fluorinated compounds in laboratory settings | Grignard reaction conducted under strictly controlled anhydrous, low-temperature conditions |
| Detection Item | Common Analytical Method | Method Overview |
|---|---|---|
| Assay (3-Fluorophenylmagnesium Bromide Content) | Acid-Base Titration with Standardized HCl | Quantifies active Grignard species by hydrolysis followed by titration of liberated Mg(OH)2 with standardized HCl. |
| Residual Solvent (THF) | Gas Chromatography (GC) with FID | Separates and quantifies THF using a polar capillary column and flame ionization detection. |
| Water Content | Karl Fischer Coulometric Titration | Measures trace water via electrochemical generation of iodine and stoichiometric reaction with water. |
| Inorganic Halides (Br-) | Potentiometric Titration with AgNO3 | Determines bromide ion concentration by argentometric titration using silver nitrate and a silver indicator electrode. |
| Metal Impurities (Fe, Ni, Cu, Pb) | ICP-OES | Simultaneously quantifies trace metal contaminants after acid digestion and nebulization into inductively coupled plasma. |
| Organic Impurities (Related Substances) | HPLC with UV Detection | Separates and detects residual starting material (3-bromofluorobenzene), biphenyl byproducts, and degradation products using reversed-phase C18 column and UV absorbance. |
| pH of Aqueous Hydrolysate | pH Meter Measurement | Measures pH of standardized aqueous hydrolyzate to assess acidity/basicity indicative of side reactions or hydrolysis extent. |
| Magnesium Content | EDTA Complexometric Titration | Determines total Mg2+ concentration by chelation with standardized EDTA under controlled pH and metallochromic indicator. |
| Appearance and Clarity | Visual Inspection in Amber Glass Vial | Assesses physical state, color, and presence of particulates or cloudiness against specified standards under controlled lighting. |
| Density | Digital Density Meter | Measures mass per unit volume at specified temperature using oscillating U-tube principle for batch consistency. |
| Residual 3-Bromofluorobenzene | GC-MS | Identifies and quantifies unreacted aryl bromide precursor using gas chromatographic separation and mass spectrometric detection. |
| Peroxide Content | Iodometric Titration | Detects peroxides by oxidation of iodide to iodine in acidic medium, followed by thiosulfate titration. |
| Test Item | Specification |
|---|---|
| Appearance | Colorless to pale yellow clear solution in tetrahydrofuran |
| Purity | >=98.5% |
| Water Content (KF) | <=0.5% |
| Total Impurities | <=1.5% |
| Single Impurity | <=0.5% |
| Identification (NMR) | Conforms to reference standard |
| Odor | Characteristic mild ether-like odor |
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| CAS/Product ID | *Required fields | |
| Lot/Batch Number | *Required fields | |
| Pictograms | ![]() ![]() |
| Signal Word | Danger |
| Safety Data Sheet | |
1. How do you ensure product quality consistency?
We rely on a mature China-based manufacturing system and implement strict batch control and quality inspection for every shipment. Our production process complies with ISO 9001 standards, and a COA is provided for each batch to ensure consistent and reliable quality.
2. Do you offer competitive pricing for bulk orders?
Yes, as a China-based manufacturer and bulk supplier, we provide tiered pricing based on order volume. We support FOB and CIF quotations, as well as L/C payment terms for large transactions to meet international trade requirements.
3. Can you support large-volume or long-term supply?
We have stable production capacity and a well-established supply chain, enabling continuous bulk supply. We support ton-level and container-level orders, as well as long-term cooperation projects.
4. What is your typical lead time?
For in-stock products, shipment can be arranged within 1–3 days. For bulk packaging or customized orders, lead time depends on the specific quantity and production schedule.
5. What documents do you provide?
We can provide complete documentation upon request, including COA, SDS, TDS, and other compliance certificates, meeting industrial procurement and export requirements.
6. Can you customize product specifications or packaging?
Yes, we support customization of parameters such as purity, impurities, residual solvents, and heavy metals. We also offer various bulk packaging options, including 25kg bags, drums, and IBC tanks, suitable for industrial applications and transportation.
7. What shipping options do you support?
We support both FCL (Full Container Load) and LCL (Less than Container Load) shipments, and can flexibly arrange logistics solutions based on order size to meet bulk chemical export needs.
8. Do you provide technical or application support?
Yes, we provide basic application guidance and technical support based on industry experience to help customers optimize product usage.
9. How do you handle compliance and export regulations?
We are familiar with international trade and export regulations, ensuring all products comply with relevant requirements. We also provide complete documentation to support smooth customs clearance and global delivery.