China Factory Direct
|
|
| CAS number | 188815-32-9 |
| Product name | 3-BROMO-5-IODOBENZOIC ACID |
| Stock | Stock readily available; annual supply capacity exceeding 1,000 tons. |
| Grade | Agricultural GradeMaterial GradeSpecialty Grade |
| Packaging | 25KG/bag500KG/bag1000KG/bag |
| Sample | Test Samples Available (Click to Request Samples) |
| COA | View COA |
| Price | Get Quote |
| Supply Type | Bulk / Contract manufacturing / OEM |
| Shipping | FCL / LCL available |
| Payment Terms | Support FOB \ CIF \ EXW quotations, and accept Letter of Credit (L/C). |
| Manufacturer | Greenrock Chemical(China Factory) |
Based on current marketvolatility and material availability.
17+ years in chemical exports.Fully compliant, reliable supply.Your B2B partner in bulk chemical procurement.
| Industry | Application | Process |
|---|---|---|
| Pharmaceuticals | Intermediate for synthesizing antitumor agents | Used in Grignard reactions and substitution reactions |
| Agrochemicals | Intermediate for synthesizing herbicides | Used in alkylation reactions and esterification reactions |
| Materials Science | Precursor for synthesizing optoelectronic materials | Applied in cross-coupling reactions and condensation reactions |
| Test Item | Common Testing Methods | Method Overview |
|---|---|---|
| Identification Test | Infrared Spectroscopy (IR) | By measuring the infrared absorption spectrum of the sample and comparing it with the standard spectrum, the characteristic functional groups of 3-bromo-5-iodobenzoic acid (such as carboxyl group, aromatic ring, C–Br, and C–I bonds) can be confirmed based on the consistency of absorption peaks. |
| Proton Nuclear Magnetic Resonance (¹H NMR) | Using ¹H NMR to determine the chemical shifts, integration areas, and coupling constants of hydrogen atoms in the sample dissolved in deuterated solvent, and compare with theoretical spectra to verify the molecular structure. | |
| Content Determination | High-Performance Liquid Chromatography (HPLC) | Use a reversed-phase C18 column, with methanol/water or acetonitrile/water as the mobile phase, and detect with a UV detector (typically at around 254 nm). Quantify the main component using external standard method or internal standard method. |
| Acid-Base Titration | Utilize the carboxylic acid group of 3-bromo-5-iodobenzoic acid for non-aqueous or aqueous titration with a standardized sodium hydroxide solution. Determine the endpoint by phenolphthalein or potentiometry to calculate purity. | |
| Related Substances (Impurity) Check | High-Performance Liquid Chromatography (HPLC) | Separate and detect possible organic impurities (such as unreacted raw materials, by-products, degradation products) using gradient elution or isocratic elution conditions. Control the limits of each impurity using area normalization or correction factor methods. |
| Drying Loss | Thermogravimetric Analysis (TGA) or Atmospheric Drying Method | Dry the sample at a specified temperature (e.g., 105°C) until constant weight, and measure the mass loss to evaluate the content of moisture and volatile substances. |
| Ignited Residue | High-Temperature Ignition Method | Ignite the sample at high temperature (usually 700–800°C), then weigh the residual inorganic material to control the total amount of inorganic impurities. |
| Bromine and Iodine Content | Elemental Analysis (EA) or Ion Chromatography (IC) | Elemental analyzer determines total halogen content; or after oxygen bottle combustion, ion chromatography is used to determine bromide and iodide ion concentrations, verifying that the halogen ratio meets the molecular formula requirements. |
| Melting Point | Capillary Melting Point Determination Method | Determine the melting range from initial melting to final melting using a melting point apparatus, and compare with literature values (approximately 220–225°C, depending on the literature) to assess purity and crystalline consistency. |
| Test Item | Specification |
|---|---|
| Appearance | Pale-yellow solid |
| Purity | >=98.0% (by LC-MS) |
| Melting Point | 172–176 °C |
| Total Impurities | <=2.0% |
| Single Impurity | <=0.5% |
| Water Content (KF) | <=0.5% |
| Heavy Metals | <=20 ppm |
| Residue on Ignition | <=0.1% |
|
|
|
| CAS/Product ID | *Required fields | |
| Lot/Batch Number | *Required fields | |
1. How do you ensure product quality consistency?
We rely on a mature China-based manufacturing system and implement strict batch control and quality inspection for every shipment. Our production process complies with ISO 9001 standards, and a COA is provided for each batch to ensure consistent and reliable quality.
2. Do you offer competitive pricing for bulk orders?
Yes, as a China-based manufacturer and bulk supplier, we provide tiered pricing based on order volume. We support FOB and CIF quotations, as well as L/C payment terms for large transactions to meet international trade requirements.
3. Can you support large-volume or long-term supply?
We have stable production capacity and a well-established supply chain, enabling continuous bulk supply. We support ton-level and container-level orders, as well as long-term cooperation projects.
4. What is your typical lead time?
For in-stock products, shipment can be arranged within 1–3 days. For bulk packaging or customized orders, lead time depends on the specific quantity and production schedule.
5. What documents do you provide?
We can provide complete documentation upon request, including COA, SDS, TDS, and other compliance certificates, meeting industrial procurement and export requirements.
6. Can you customize product specifications or packaging?
Yes, we support customization of parameters such as purity, impurities, residual solvents, and heavy metals. We also offer various bulk packaging options, including 25kg bags, drums, and IBC tanks, suitable for industrial applications and transportation.
7. What shipping options do you support?
We support both FCL (Full Container Load) and LCL (Less than Container Load) shipments, and can flexibly arrange logistics solutions based on order size to meet bulk chemical export needs.
8. Do you provide technical or application support?
Yes, we provide basic application guidance and technical support based on industry experience to help customers optimize product usage.
9. How do you handle compliance and export regulations?
We are familiar with international trade and export regulations, ensuring all products comply with relevant requirements. We also provide complete documentation to support smooth customs clearance and global delivery.