China Factory Direct
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| CAS number | 3430-13-5 |
| Product name | 5-Bromo-2-methylpyridine |
| Stock | Stock readily available; annual supply capacity exceeding 1,000 tons. |
| Grade | Agricultural GradeReagent GradeIndustrial GradeSpecialty Grade |
| Packaging | 25KG/bag500KG/bag1000KG/bag |
| Sample | Test Samples Available (Click to Request Samples) |
| COA | View COA |
| Price | Get Quote |
| Supply Type | Bulk / Contract manufacturing / OEM |
| Shipping | FCL / LCL available |
| Payment Terms | Support FOB \ CIF \ EXW quotations, and accept Letter of Credit (L/C). |
| Manufacturer | Greenrock Chemical(China Factory) |
Based on current marketvolatility and material availability.
17+ years in chemical exports.Fully compliant, reliable supply.Your B2B partner in bulk chemical procurement.
| Industry | Application | Process |
|---|---|---|
| Pharmaceutical Industry | Intermediate | Used in the synthesis of pharmaceuticals for treating certain diseases |
| Agrochemical Industry | Intermediate | Used in the synthesis of pesticides |
| Organic Synthesis | Raw material for synthesizing other compounds | Serves as a starting material for synthesizing other nitrogen-containing heterocyclic compounds |
| Research | Chemical research | Applied in laboratory-scale chemical reaction studies |
| Detection Item | Common Testing Methods | Method Overview |
|---|---|---|
| Appearance and Physical Properties | Visual Inspection + Physical Property Measurement | Observe sample color and state (typically colorless to pale yellow liquid or low-melting solid); determine melting point or boiling point range, conforming to pharmacopoeia or company specifications. |
| Purity (Main Component Content) | High-Performance Liquid Chromatography (HPLC) | Use C18 column with methanol-water or acetonitrile-water as mobile phase, UV detector (254 nm), external standard or internal standard method for quantification; typically requires ≥98.0%. |
| Impurity Profile Analysis | HPLC (Impurity Detection) | Same HPLC method, reduce detection wavelength or use gradient elution to separate and quantify known impurities (e.g., unreacted starting materials, debromination products, oxidation by-products), controlled per ICH Q3B guidelines for individual and total impurity limits. |
| Residual Solvents | Gas Chromatography (GC) | Use headspace or direct injection, DB-624 or HP-INNOWAX column, FID detector; detect residual solvents such as methanol, ethanol, acetone, dichloromethane according to ICH Q3C guidelines. |
| Moisture Content | Karl Fischer Titration | Use coulometric or volumetric Karl Fischer reagent to accurately measure trace water content; control moisture at ≤0.5% (adjustable based on application) to prevent hydrolysis or instability. |
| Bromine Content | Combustion Ion Chromatography / X-ray Fluorescence (XRF) | Determine bromide ions in combustion-derived solution via ion chromatography, or non-destructively measure bromine content using XRF; verify bromine atom ratio matches theoretical value (theoretical Br ≈ 50.2%). |
| Melting Point / Boiling Point | Melting Point Apparatus / Boiling Point Determination Device | Determine melting point (literature value ~35–40°C) or atmospheric boiling point (~210–215°C), serving as physical constants for identification and purity assessment. |
| UV-Visible Absorption Spectroscopy | UV-Vis Spectrophotometry | Dissolve sample in ethanol or methanol, measure absorption spectrum from 200–400 nm; characteristic absorption peak around 260–270 nm used for preliminary identification and concentration estimation. |
| Nuclear Magnetic Resonance (¹H NMR) | Proton Nuclear Magnetic Resonance | Use CDCl₃ as solvent; confirm molecular structure and identify impurities via chemical shifts (e.g., 2-CH₃: δ ≈ 2.5 ppm; Ar-H: δ ≈ 7.2–8.0 ppm) and integration ratios. |
| Gas Chromatography-Mass Spectrometry (GC-MS) | GC-MS | Used for qualitative analysis of unknown impurities; match mass spectral fragments against databases (e.g., NIST) to identify potential degradation products or synthetic by-products. |
| Test Item | Specification |
|---|---|
| Appearance | White to light yellow or green powder to lump |
| Purity | >=98.0% (HPLC) |
| Total Impurities | <=2.0% |
| Single Impurity | <=0.5% |
| Water Content (KF) | <=0.5% |
| Melting Point | 52–56°C |
| Identification (NMR) | Consistent with structure |
| Identification (IR) | Consistent with structure |
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| CAS/Product ID | *Required fields | |
| Lot/Batch Number | *Required fields | |
1. How do you ensure product quality consistency?
We rely on a mature China-based manufacturing system and implement strict batch control and quality inspection for every shipment. Our production process complies with ISO 9001 standards, and a COA is provided for each batch to ensure consistent and reliable quality.
2. Do you offer competitive pricing for bulk orders?
Yes, as a China-based manufacturer and bulk supplier, we provide tiered pricing based on order volume. We support FOB and CIF quotations, as well as L/C payment terms for large transactions to meet international trade requirements.
3. Can you support large-volume or long-term supply?
We have stable production capacity and a well-established supply chain, enabling continuous bulk supply. We support ton-level and container-level orders, as well as long-term cooperation projects.
4. What is your typical lead time?
For in-stock products, shipment can be arranged within 1–3 days. For bulk packaging or customized orders, lead time depends on the specific quantity and production schedule.
5. What documents do you provide?
We can provide complete documentation upon request, including COA, SDS, TDS, and other compliance certificates, meeting industrial procurement and export requirements.
6. Can you customize product specifications or packaging?
Yes, we support customization of parameters such as purity, impurities, residual solvents, and heavy metals. We also offer various bulk packaging options, including 25kg bags, drums, and IBC tanks, suitable for industrial applications and transportation.
7. What shipping options do you support?
We support both FCL (Full Container Load) and LCL (Less than Container Load) shipments, and can flexibly arrange logistics solutions based on order size to meet bulk chemical export needs.
8. Do you provide technical or application support?
Yes, we provide basic application guidance and technical support based on industry experience to help customers optimize product usage.
9. How do you handle compliance and export regulations?
We are familiar with international trade and export regulations, ensuring all products comply with relevant requirements. We also provide complete documentation to support smooth customs clearance and global delivery.