China Factory Direct
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| CAS number | 4111-55-1 |
| Product name | LITHIUM DICYCLOHEXYLAMIDE |
| Stock | Stock readily available; annual supply capacity exceeding 1,000 tons. |
| Grade | Pharmaceutical GradeMaterial GradeSpecialty Grade |
| Packaging | 25KG/bag |
| Sample | Test Samples Available (Click to Request Samples) |
| COA | View COA |
| Price | Get Quote |
| Supply Type | Bulk / Contract manufacturing / OEM |
| Shipping | FCL / LCL available |
| Payment Terms | Support FOB \ CIF \ EXW quotations, and accept Letter of Credit (L/C). |
| Manufacturer | Greenrock Chemical(China Factory) |
Based on current marketvolatility and material availability.
17+ years in chemical exports.Fully compliant, reliable supply.Your B2B partner in bulk chemical procurement.
| Industry | Application | Process |
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| Organic Synthesis | Used as a strong base for deprotonation reactions, particularly lithiation of weakly acidic substrates (e.g., hydrocarbons, sulfonamides) | Reacted with substrates under anhydrous and oxygen-free conditions in low-boiling solvents such as tetrahydrofuran (THF) or diethyl ether at low temperatures (e.g., –78 °C) to generate the corresponding organolithium reagents |
| Pharmaceutical Intermediates Synthesis | Employed in key lithiation steps for constructing chiral centers and heterocyclic compounds (e.g., indole and quinoline derivatives) | Directed ortho-lithiation of aromatic heterocyclic substrates containing active hydrogen, followed by electrophilic trapping (e.g., with aldehydes, ketones, or alkyl halides) to form C–C bonds |
| Materials Science | Applied as a polymerization initiator to control molecular weight and microstructure of polyolefins or specialty functional polymers | Acts synergistically with transition metal catalysts in coordination polymerization to enable living/controlled anionic polymerization |
| Detection Item | Common Analytical Method | Method Overview |
|---|---|---|
| Assay (Purity) | Acid-Base Titration with Standardized HCl | Quantifies lithium amide content by protonation with standardized hydrochloric acid and endpoint detection using potentiometric or indicator-based titration. |
| Moisture Content | Karl Fischer Coulometric Titration | Determines trace water via electrochemical generation of iodine reacting stoichiometrically with water in anhydrous methanol-based solvent. |
| Residual Solvents (e.g., THF, Hexane) | Gas Chromatography with Flame Ionization Detection (GC-FID) | Separates and quantifies volatile organic solvents based on retention time and FID response relative to calibrated standards. |
| Inorganic Chloride Impurity | Ion Chromatography with Conductivity Detection (IC-CD) | Separates chloride anions on an ion-exchange column and detects them via changes in solution conductivity. |
| Lithium Content | Inductively Coupled Plasma Optical Emission Spectrometry (ICP-OES) | Measures lithium atomic emission intensity at characteristic wavelength after high-temperature plasma atomization and excitation. |
| Heavy Metals (Pb, Cd, Hg, As) | Inductively Coupled Plasma Mass Spectrometry (ICP-MS) | Detects trace heavy metals by mass-to-charge ratio after ionization in argon plasma, offering sub-ppt sensitivity. |
| Appearance and Color | Visual Inspection against ASTM D1209 Standard | Compares sample clarity and color visually in a 100-mm cell to platinum-cobalt (APHA) color standards under controlled lighting. |
| Melting Point | Capillary Melting Point Apparatus | Determines temperature range at which solid transitions to liquid using calibrated capillary tube method per USP <741>. |
| Organic Impurities (Related Substances) | High-Performance Liquid Chromatography with UV Detection (HPLC-UV) | Separates and quantifies structurally related impurities using reversed-phase C18 column and UV absorbance at 210 nm. |
| Residue on Ignition | Gravimetric Analysis (Weight Loss on Ignition) | Measures non-volatile inorganic residue after controlled ashing at 550-600 C and subsequent weighing. |
| pH of Aqueous Slurry | Potentiometric pH Measurement | Measures hydrogen ion activity in a defined suspension (e.g., 1% w/v in CO2-free water) using calibrated glass electrode. |
| Particle Size Distribution | Laser Diffraction Particle Size Analysis | Determines size distribution by analyzing angular variation in laser light scattering intensity from dispersed particles in liquid medium. |
| Test Item | Specification |
|---|---|
| Appearance | White to off-white crystalline powder |
| Purity | >=98.5% |
| Water Content (KF) | <=0.5% |
| Melting Point | 128-132°C |
| Total Impurities | <=1.5% |
| Single Impurity | <=0.5% |
| Heavy Metals | <=20 ppm |
| Residue on Ignition | <=0.1% |
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| CAS/Product ID | *Required fields | |
| Lot/Batch Number | *Required fields | |
1. How do you ensure product quality consistency?
We rely on a mature China-based manufacturing system and implement strict batch control and quality inspection for every shipment. Our production process complies with ISO 9001 standards, and a COA is provided for each batch to ensure consistent and reliable quality.
2. Do you offer competitive pricing for bulk orders?
Yes, as a China-based manufacturer and bulk supplier, we provide tiered pricing based on order volume. We support FOB and CIF quotations, as well as L/C payment terms for large transactions to meet international trade requirements.
3. Can you support large-volume or long-term supply?
We have stable production capacity and a well-established supply chain, enabling continuous bulk supply. We support ton-level and container-level orders, as well as long-term cooperation projects.
4. What is your typical lead time?
For in-stock products, shipment can be arranged within 1–3 days. For bulk packaging or customized orders, lead time depends on the specific quantity and production schedule.
5. What documents do you provide?
We can provide complete documentation upon request, including COA, SDS, TDS, and other compliance certificates, meeting industrial procurement and export requirements.
6. Can you customize product specifications or packaging?
Yes, we support customization of parameters such as purity, impurities, residual solvents, and heavy metals. We also offer various bulk packaging options, including 25kg bags, drums, and IBC tanks, suitable for industrial applications and transportation.
7. What shipping options do you support?
We support both FCL (Full Container Load) and LCL (Less than Container Load) shipments, and can flexibly arrange logistics solutions based on order size to meet bulk chemical export needs.
8. Do you provide technical or application support?
Yes, we provide basic application guidance and technical support based on industry experience to help customers optimize product usage.
9. How do you handle compliance and export regulations?
We are familiar with international trade and export regulations, ensuring all products comply with relevant requirements. We also provide complete documentation to support smooth customs clearance and global delivery.