China Factory Direct
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| CAS number | 480438-50-4 |
| Product name | 3-CHLORO-5-FLUOROPHENYLMAGNESIUM BROMIDE |
| Stock | Stock readily available; annual supply capacity exceeding 1,000 tons. |
| Grade | Agricultural GradePharmaceutical GradeMaterial GradeSpecialty Grade |
| Packaging | 25KG/bag |
| Sample | Test Samples Available (Click to Request Samples) |
| COA | View COA |
| Price | Get Quote |
| Supply Type | Bulk / Contract manufacturing / OEM |
| Shipping | FCL / LCL available |
| Payment Terms | Support FOB \ CIF \ EXW quotations, and accept Letter of Credit (L/C). |
| Manufacturer | Greenrock Chemical(China Factory) |
Based on current marketvolatility and material availability.
17+ years in chemical exports.Fully compliant, reliable supply.Your B2B partner in bulk chemical procurement.
| Industry | Application | Process |
|---|---|---|
| Pharmaceuticals | Synthesis of antitumor drug intermediates | Grignard reagent coupling reaction |
| Agrochemicals | Preparation of fluorinated pesticide intermediates | Substitution or cross-coupling reaction |
| Materials | Synthesis of high-performance fluorinated polymer monomers | Introduction of fluorochloro groups into polymer precursors |
| Pharmaceutical R&D | Tool for probe compound synthesis | Nucleophilic reagent in organic synthesis |
| Detection Item | Common Analytical Method | Method Overview |
|---|---|---|
| Assay (Main Component Content) | Gas Chromatography (GC) with Flame Ionization Detection (FID) | Quantifies 3-chloro-5-fluorophenylmagnesium bromide via derivatization (e.g., quenching with methanol followed by GC analysis of the corresponding aryl methyl ether) using external standard calibration. |
| Residual Solvents (THF, Diethyl Ether) | Headspace Gas Chromatography (HS-GC) | Measures volatile solvents co-dissolved in the Grignard reagent solution by equilibrium headspace sampling and separation on a polar capillary column. |
| Water Content | Karl Fischer Titration (Coulometric mode) | Determines trace water by electrochemical generation of iodine reacting stoichiometrically with water in anhydrous methanol-based reagent. |
| Heavy Metals (Pb, Cd, Hg, As) | Inductively Coupled Plasma Mass Spectrometry (ICP-MS) | Quantifies trace metallic impurities after acid digestion and dilution; offers sub-ppt detection limits and multi-element capability. |
| Chloride Ion Impurity | Ion Chromatography (IC) with Conductivity Detection | Separates and quantifies Cl⁻ anions using anion-exchange column and suppressed conductivity detection after sample neutralization and dilution. |
| Residual Magnesium | Inductively Coupled Plasma Optical Emission Spectrometry (ICP-OES) | Measures total Mg concentration post-acid digestion to verify stoichiometric consistency and detect excess or depleted magnesium. |
| Appearance and Color | Visual Inspection against ASTM D1209 Standard | Assesses solution clarity and color (APHA/Pt-Co scale) in standardized glass cells under controlled lighting to detect decomposition or particulate contamination. |
| pH (after controlled hydrolysis) | Potentiometric pH Measurement | Evaluates acidity/basicity of the aqueous hydrolysate to infer presence of acidic or basic degradation products (e.g., HBr, Mg(OH)₂). |
| Test Item | Specification |
|---|---|
| Appearance | Colorless to pale yellow clear solution in tetrahydrofuran |
| Purity | >=98.5% |
| Water Content (KF) | <=0.5% |
| Total Impurities | <=1.5% |
| Single Impurity | <=0.3% |
| Identification (NMR) | Conforms to reference standard |
| Odor | Characteristic mild ether-like odor |
| Solubility | Miscible with THF, diethyl ether; insoluble in water |
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| CAS/Product ID | *Required fields | |
| Lot/Batch Number | *Required fields | |
| Pictograms | ![]() |
| Signal Word | Warning |
| Safety Data Sheet | |
1. How do you ensure product quality consistency?
We rely on a mature China-based manufacturing system and implement strict batch control and quality inspection for every shipment. Our production process complies with ISO 9001 standards, and a COA is provided for each batch to ensure consistent and reliable quality.
2. Do you offer competitive pricing for bulk orders?
Yes, as a China-based manufacturer and bulk supplier, we provide tiered pricing based on order volume. We support FOB and CIF quotations, as well as L/C payment terms for large transactions to meet international trade requirements.
3. Can you support large-volume or long-term supply?
We have stable production capacity and a well-established supply chain, enabling continuous bulk supply. We support ton-level and container-level orders, as well as long-term cooperation projects.
4. What is your typical lead time?
For in-stock products, shipment can be arranged within 1–3 days. For bulk packaging or customized orders, lead time depends on the specific quantity and production schedule.
5. What documents do you provide?
We can provide complete documentation upon request, including COA, SDS, TDS, and other compliance certificates, meeting industrial procurement and export requirements.
6. Can you customize product specifications or packaging?
Yes, we support customization of parameters such as purity, impurities, residual solvents, and heavy metals. We also offer various bulk packaging options, including 25kg bags, drums, and IBC tanks, suitable for industrial applications and transportation.
7. What shipping options do you support?
We support both FCL (Full Container Load) and LCL (Less than Container Load) shipments, and can flexibly arrange logistics solutions based on order size to meet bulk chemical export needs.
8. Do you provide technical or application support?
Yes, we provide basic application guidance and technical support based on industry experience to help customers optimize product usage.
9. How do you handle compliance and export regulations?
We are familiar with international trade and export regulations, ensuring all products comply with relevant requirements. We also provide complete documentation to support smooth customs clearance and global delivery.