China Factory Direct
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| CAS number | 6320-03-2 |
| Product name | 2-CHLOROTHIOPHENOL |
| Stock | Stock readily available; annual supply capacity exceeding 1,000 tons. |
| Grade | Pharmaceutical GradeIndustrial GradeSpecialty GradeMaterial Grade |
| Packaging | 25L/drum200L/drum1000L/IBC |
| Sample | Test Samples Available (Click to Request Samples) |
| COA | View COA |
| Price | Get Quote |
| Supply Type | Bulk / Contract manufacturing / OEM |
| Shipping | FCL / LCL available |
| Payment Terms | Support FOB \ CIF \ EXW quotations, and accept Letter of Credit (L/C). |
| Manufacturer | Greenrock Chemical(China Factory) |
Based on current marketvolatility and material availability.
17+ years in chemical exports.Fully compliant, reliable supply.Your B2B partner in bulk chemical procurement.
| Industry | Application | Process |
|---|---|---|
| Pesticides | Key intermediate for synthesizing organophosphorus insecticides (e.g., chlorpyrifos, methyl chlorpyrifos) | Reacted with phosphorus oxychloride or diethylamine, followed by cyclization and substitution to produce target pesticides |
| Pharmaceuticals | Intermediate for synthesizing antibacterial agents (e.g., sulfonamide derivatives) and antitumor drugs | Used in coupling reactions or as a thioetherification reagent to construct sulfur-containing heterocyclic structures |
| Dyes | Used to synthesize benzothiazole-based fluorescent brighteners and thioindigo dyes | Condensed with aldehydes to form the benzothiazole ring, or serves as a sulfur source in dye molecule synthesis |
| Rubber additives | Raw material for producing rubber accelerators (e.g., CBS, TBBS) | Reacted with cyclohexylamine and carbon disulfide to generate benzothiazole-based accelerators |
| Test Item | Common Testing Methods | Method Overview |
|---|---|---|
| Purity and Content Determination | High-Performance Liquid Chromatography (HPLC) | Uses a C18 reversed-phase column, with methanol/water or acetonitrile/water as the mobile phase. Detection is performed using a UV detector (254 nm). The content of o-chlorobenzenethiol is quantified by external or internal standard methods, offering good resolution and high accuracy. |
| Purity and Content Determination | Gas Chromatography (GC) | Employs a capillary column (e.g., DB-5) with an FID detector. Temperature programming is used for separation, suitable for samples with good volatility. Thermal stability should be considered to avoid decomposition. |
| Impurity Analysis | HPLC-MS / GC-MS | Mass spectrometry coupled methods can qualitatively and quantitatively detect process-related impurities (e.g., dimers, o-chlorophenol, unreacted starting material such as chlorobenzene), providing molecular weight and structural information with high sensitivity. |
| Moisture Determination | Karl Fischer Titration | Suitable for trace moisture analysis with high accuracy. Used to control trace water content in o-chlorobenzenethiol. Interference from sulfur-containing compounds should be avoided; appropriate solvents (e.g., methanol-pyridine system) should be selected. |
| Sulfur Content Determination | Oxygen Flask Combustion - Ion Chromatography / Combustion Iodometry | The sample is completely combusted in an oxygen flask, converting sulfur to sulfate. Sulfate is measured by ion chromatography or titrated using iodometry, to confirm whether the sulfur content meets the theoretical value (approximately 34.5%). |
| Appearance and Color | Visual Inspection / Color Measurement (APHA) | Observe sample as a colorless to pale yellow liquid. APHA colorimeter or color chart is used to assess color intensity, indicating the presence of oxidative or polymeric impurities. |
| pH Value (aqueous solution) | pH Meter Measurement | Dissolve the sample in an appropriate amount of water (or ethanol-water mixture), and measure the pH using a calibrated pH meter. O-Chlorobenzenethiol is weakly acidic (pH ≈ 5–6), useful for detecting alkaline impurities. |
| Boiling Point/Distillation Range | Distillation Method / Boiling Point Apparatus | Determine the atmospheric boiling point (approximately 215–218 °C) to assess purity. A wide distillation range or presence of low-boiling impurities suggests residual solvents or by-products. |
| Heavy Metal Residues | Atomic Absorption Spectroscopy (AAS) or ICP-MS | After sample digestion, determine the content of heavy metals such as lead, cadmium, mercury, and arsenic, ensuring compliance with pharmacopoeia or chemical standards (e.g., ICH Q3D limits). |
| Chlorine Content Determination | Combustion Ion Chromatography / Coulometric Titration | After combustion, chlorine is converted to chloride ions and quantified by ion chromatography, or measured using coulometric titration for total chlorine content, verifying whether the chlorine content matches the theoretical value (approximately 43.8%). |
| Test Item | Specification |
|---|---|
| Appearance | Pale yellow to amber liquid |
| Purity | >=98.5% |
| Water Content (KF) | <=0.5% |
| Total Impurities | <=1.5% |
| Single Impurity | <=0.3% |
| Refractive Index (n20/D) | 1.625–1.635 |
| Relative Density (20°C/25°C) | 1.270–1.290 g/cm³ |
| Odor | Characteristic pungent odor |
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| CAS/Product ID | *Required fields | |
| Lot/Batch Number | *Required fields | |
1. How do you ensure product quality consistency?
We rely on a mature China-based manufacturing system and implement strict batch control and quality inspection for every shipment. Our production process complies with ISO 9001 standards, and a COA is provided for each batch to ensure consistent and reliable quality.
2. Do you offer competitive pricing for bulk orders?
Yes, as a China-based manufacturer and bulk supplier, we provide tiered pricing based on order volume. We support FOB and CIF quotations, as well as L/C payment terms for large transactions to meet international trade requirements.
3. Can you support large-volume or long-term supply?
We have stable production capacity and a well-established supply chain, enabling continuous bulk supply. We support ton-level and container-level orders, as well as long-term cooperation projects.
4. What is your typical lead time?
For in-stock products, shipment can be arranged within 1–3 days. For bulk packaging or customized orders, lead time depends on the specific quantity and production schedule.
5. What documents do you provide?
We can provide complete documentation upon request, including COA, SDS, TDS, and other compliance certificates, meeting industrial procurement and export requirements.
6. Can you customize product specifications or packaging?
Yes, we support customization of parameters such as purity, impurities, residual solvents, and heavy metals. We also offer various bulk packaging options, including 25kg bags, drums, and IBC tanks, suitable for industrial applications and transportation.
7. What shipping options do you support?
We support both FCL (Full Container Load) and LCL (Less than Container Load) shipments, and can flexibly arrange logistics solutions based on order size to meet bulk chemical export needs.
8. Do you provide technical or application support?
Yes, we provide basic application guidance and technical support based on industry experience to help customers optimize product usage.
9. How do you handle compliance and export regulations?
We are familiar with international trade and export regulations, ensuring all products comply with relevant requirements. We also provide complete documentation to support smooth customs clearance and global delivery.