China Factory Direct
|
|
| CAS number | 64168-34-9 |
| Product name | 3-FLUOROBENZYLMAGNESIUM CHLORIDE |
| Stock | Stock readily available; annual supply capacity exceeding 1,000 tons. |
| Grade | Agricultural GradeIndustrial GradeSpecialty Grade |
| Packaging | 25KG/bag |
| Sample | Test Samples Available (Click to Request Samples) |
| COA | View COA |
| Price | Get Quote |
| Supply Type | Bulk / Contract manufacturing / OEM |
| Shipping | FCL / LCL available |
| Payment Terms | Support FOB \ CIF \ EXW quotations, and accept Letter of Credit (L/C). |
| Manufacturer | Greenrock Chemical(China Factory) |
Based on current marketvolatility and material availability.
17+ years in chemical exports.Fully compliant, reliable supply.Your B2B partner in bulk chemical procurement.
| Industry | Application | Process |
|---|---|---|
| Pharmaceuticals | Synthesis of fluorinated pharmaceutical intermediates | Used as a Grignard reagent in nucleophilic addition reactions with carbonyl compounds (e.g., aldehydes, ketones) to construct C–C bonds for preparing 3-fluoro-phenylethanol derivatives |
| Pesticides | Synthesis of fluorinated fungicide/insecticide intermediates | Reacted with ethylene oxide or aldehydes to introduce fluorinated side chains for constructing bioactive molecular scaffolds |
| Chemical Synthesis | Synthesis of fluorinated aryl ketones or alcohols | Reacted with nitriles, esters, or carbon dioxide, followed by hydrolysis or acidification to yield corresponding carboxylic acids, ketones, or alcohols |
| Detection Item | Common Analytical Method | Method Overview |
|---|---|---|
| Assay (3-Fluorobenzylmagnesium Chloride) | Acid-Base Titration with Standardized HCl | Quantifies active Grignard species by acid hydrolysis followed by back-titration of excess acid. |
| Moisture Content | Karl Fischer Titration | Measures water content via coulometric or volumetric reaction between water and iodine/sulfur dioxide in pyridine-methanol medium. |
| Residual Solvent (THF) | Gas Chromatography (GC) with FID | Separates and quantifies tetrahydrofuran using a capillary column and flame ionization detection. |
| Heavy Metals (Pb, Cd, Hg, Cr) | ICP-OES | Simultaneously detects trace metal impurities after acid digestion by measuring element-specific atomic emission intensities. |
| Chloride Ion Impurity | Potentiometric Titration with AgNO3 | Determines free chloride via silver nitrate titration monitored by silver ion-selective electrode endpoint detection. |
| 3-Fluorobenzyl Alcohol (Hydrolysis Byproduct) | GC-MS | Identifies and quantifies the alcohol degradation product using gas chromatographic separation coupled with mass spectral detection. |
| 3-Fluorotoluene (Reduction Byproduct) | GC-FID | Detects and quantifies this organic impurity by retention time matching and peak area comparison against reference standard. |
| Magnesium Content | Atomic Absorption Spectroscopy (AAS) | Measures total magnesium concentration by absorption of characteristic radiation from a magnesium hollow cathode lamp. |
| pH of Aqueous Hydrolysate | pH Meter Measurement | Evaluates acidity/basicity of the aqueous phase after controlled hydrolysis to assess residual basicity or acidic impurities. |
| Appearance and Clarity | Visual Inspection | Assesses physical state, color, and presence of suspended particles or phase separation under controlled lighting conditions. |
| Density | Digital Density Meter | Determines mass per unit volume at specified temperature using oscillating U-tube principle. |
| Reactivity Test (with CO2 or Benzaldehyde) | Qualitative Reaction Monitoring | Confirms functional Grignard activity by observing expected precipitate formation or exothermic response upon addition of electrophile. |
| Test Item | Specification |
|---|---|
| Appearance | Colorless to pale yellow liquid |
| Purity | >=98.5% |
| Water Content (KF) | <=0.5% |
| Total Impurities | <=1.5% |
| Single Impurity | <=0.5% |
| Identification (NMR) | Conforms to reference standard |
| Refractive Index (n20/D) | 1.515–1.525 |
| Relative Density (20°C/25°C) | 1.22–1.26 g/cm³ |
|
|
|
| CAS/Product ID | *Required fields | |
| Lot/Batch Number | *Required fields | |
1. How do you ensure product quality consistency?
We rely on a mature China-based manufacturing system and implement strict batch control and quality inspection for every shipment. Our production process complies with ISO 9001 standards, and a COA is provided for each batch to ensure consistent and reliable quality.
2. Do you offer competitive pricing for bulk orders?
Yes, as a China-based manufacturer and bulk supplier, we provide tiered pricing based on order volume. We support FOB and CIF quotations, as well as L/C payment terms for large transactions to meet international trade requirements.
3. Can you support large-volume or long-term supply?
We have stable production capacity and a well-established supply chain, enabling continuous bulk supply. We support ton-level and container-level orders, as well as long-term cooperation projects.
4. What is your typical lead time?
For in-stock products, shipment can be arranged within 1–3 days. For bulk packaging or customized orders, lead time depends on the specific quantity and production schedule.
5. What documents do you provide?
We can provide complete documentation upon request, including COA, SDS, TDS, and other compliance certificates, meeting industrial procurement and export requirements.
6. Can you customize product specifications or packaging?
Yes, we support customization of parameters such as purity, impurities, residual solvents, and heavy metals. We also offer various bulk packaging options, including 25kg bags, drums, and IBC tanks, suitable for industrial applications and transportation.
7. What shipping options do you support?
We support both FCL (Full Container Load) and LCL (Less than Container Load) shipments, and can flexibly arrange logistics solutions based on order size to meet bulk chemical export needs.
8. Do you provide technical or application support?
Yes, we provide basic application guidance and technical support based on industry experience to help customers optimize product usage.
9. How do you handle compliance and export regulations?
We are familiar with international trade and export regulations, ensuring all products comply with relevant requirements. We also provide complete documentation to support smooth customs clearance and global delivery.