4-Nitrobenzyl 2-diazoacetoacetate Bulk Supply for Industrial Use
China Factory Direct
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| CAS number | 82551-63-1 |
| Product name | 4-Nitrobenzyl 2-diazoacetoacetate |
| Stock | Stock readily available; annual supply capacity exceeding 1,000 tons. |
| Grade | Pharmaceutical GradeMaterial GradeSpecialty GradeIndustrial Grade |
| Packaging | 25KG/bag500KG/bag1000KG/bag |
| Sample | Test Samples Available (Click to Request Samples) |
| COA | View COA |
| Price | Get Quote |
| Supply Type | Bulk / Contract manufacturing / OEM |
| Shipping | FCL / LCL available |
| Payment Terms | Support FOB \ CIF \ EXW quotations, and accept Letter of Credit (L/C). |
| Manufacturer | Greenrock Chemical(China Factory) |
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Documents We Provide for 4-Nitrobenzyl 2-diazoacetoacetate
Post-sale: Full documentation is provided.
To request documents, please contact us via email at sales@GRchemical.com.
Bulk 4-Nitrobenzyl 2-diazoacetoacetate Supplier from China
17+ years in chemical exports.Fully compliant, reliable supply.Your B2B partner in bulk chemical procurement.
Industrial Applications of 4-Nitrobenzyl 2-diazoacetoacetate
| Industry | Application | Process |
|---|---|---|
| Organic Synthesis | Intermediate for synthesizing pharmaceuticals and functional molecules | Used in diazotization coupling with ethyl acetoacetate p-nitrobenzyl ester to construct complex organic structures |
| Pharmaceutical R&D | Precursor for synthesizing antitumor agents and bioactive compounds | Applied in molecular modification and targeted synthesis leveraging the reactivity of its diazo group |
| Polymer Materials | Preparation of photoinitiators or crosslinking agents | Releases nitrogen gas under UV irradiation to initiate polymerization or crosslinking reactions |
| Fine Chemicals | Participation as a photochemical reagent in controlled synthesis reactions | Enables selective reactions under specific-wavelength light exposure, based on its photolytic properties |
Manufacturing Quality Control of 4-Nitrobenzyl 2-diazoacetoacetate
| Detection Item | Common Analytical Method | Method Overview |
|---|---|---|
| Assay (Purity) | HPLC-UV | Quantifies main compound using reversed-phase HPLC with UV detection at 254 nm, based on peak area comparison against reference standard. |
| Related Substances | HPLC-UV | Detects and quantifies structurally related impurities (e.g., diazo decomposition products, hydrolysis by-products) using gradient HPLC-UV. |
| Residual Solvents | GC-FID | Measures residual solvents (e.g., ethyl acetate, toluene, methanol) by gas chromatography with flame ionization detection using headspace sampling. |
| Water Content | Karl Fischer Titration | Determines trace water by coulometric or volumetric titration with iodine generated electrochemically in pyridine-free reagent. |
| Heavy Metals | ICP-OES | Quantifies Pb, Cd, Hg, As, and other regulated metals after acid digestion, using inductively coupled plasma optical emission spectrometry. |
| Chloride Impurity | Ion Chromatography | Separates and quantifies chloride ions using suppressed conductivity detection after aqueous extraction. |
| Residual Palladium | ICP-MS | Detects trace palladium catalyst residues post-hydrogenation via microwave-assisted digestion followed by inductively coupled plasma mass spectrometry. |
| Melting Point | Capillary Melting Point Apparatus | Determines temperature range of solid-to-liquid transition using calibrated capillary apparatus per USP <741>. |
| Appearance | Visual Inspection | Assesses physical state, color, and presence of foreign particles under controlled white light against standard reference. |
| Loss on Drying | Gravimetric Analysis | Measures volatile content by weight loss after drying at 60 C under vacuum for 2 hours. |
| Acid Value | Acid-Base Titration | Quantifies free acidic impurities by titration with standardized KOH ethanol solution using phenolphthalein indicator. |
| Specific Optical Rotation | Polarimetry | Measures chiral purity (if applicable) using sodium D-line light at specified concentration and path length in chloroform. |
Technical Specifications of 4-Nitrobenzyl 2-diazoacetoacetate
| Test Item | Specification |
|---|---|
| Appearance | Pale Yellow to Light Yellow Solid |
| Purity | >=98.0% (LC-MS) |
| Total Impurities | <=2.0% |
| Single Impurity | <=0.5% |
| Water Content (KF) | <=0.5% |
| Melting Point | 75–79°C |
| Identification (NMR) | Conforms to reference spectrum |
| Heavy Metals | <=10 ppm |
Specifications vary by industry. Reach out to our technical experts for a COA tailored specifically to your application. Email:selse@GRchemical.com
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Download COA of 4-Nitrobenzyl 2-diazoacetoacetate
| CAS/Product ID | *Required fields | |
| Lot/Batch Number | *Required fields | |
NMR Spectra of 4-Nitrobenzyl 2-diazoacetoacetate
Packaging of 4-Nitrobenzyl 2-diazoacetoacetate
Industrial 4-Nitrobenzyl 2-diazoacetoacetate Procurement FAQ
1. How do you ensure product quality consistency?
We rely on a mature China-based manufacturing system and implement strict batch control and quality inspection for every shipment. Our production process complies with ISO 9001 standards, and a COA is provided for each batch to ensure consistent and reliable quality.
2. Do you offer competitive pricing for bulk orders?
Yes, as a China-based manufacturer and bulk supplier, we provide tiered pricing based on order volume. We support FOB and CIF quotations, as well as L/C payment terms for large transactions to meet international trade requirements.
3. Can you support large-volume or long-term supply?
We have stable production capacity and a well-established supply chain, enabling continuous bulk supply. We support ton-level and container-level orders, as well as long-term cooperation projects.
4. What is your typical lead time?
For in-stock products, shipment can be arranged within 1–3 days. For bulk packaging or customized orders, lead time depends on the specific quantity and production schedule.
5. What documents do you provide?
We can provide complete documentation upon request, including COA, SDS, TDS, and other compliance certificates, meeting industrial procurement and export requirements.
6. Can you customize product specifications or packaging?
Yes, we support customization of parameters such as purity, impurities, residual solvents, and heavy metals. We also offer various bulk packaging options, including 25kg bags, drums, and IBC tanks, suitable for industrial applications and transportation.
7. What shipping options do you support?
We support both FCL (Full Container Load) and LCL (Less than Container Load) shipments, and can flexibly arrange logistics solutions based on order size to meet bulk chemical export needs.
8. Do you provide technical or application support?
Yes, we provide basic application guidance and technical support based on industry experience to help customers optimize product usage.
9. How do you handle compliance and export regulations?
We are familiar with international trade and export regulations, ensuring all products comply with relevant requirements. We also provide complete documentation to support smooth customs clearance and global delivery.
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