China Factory Direct
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| CAS number | 84624-17-9 |
| Product name | FMOC-D-Valine |
| Stock | Stock readily available; annual supply capacity exceeding 1,000 tons. |
| Grade | Pharmaceutical GradeMaterial GradeSpecialty GradeReagent GradeIndustrial Grade |
| Packaging | 25KG/bag500KG/bag1000KG/bag |
| Sample | Test Samples Available (Click to Request Samples) |
| COA | View COA |
| Price | Get Quote |
| Supply Type | Bulk / Contract manufacturing / OEM |
| Shipping | FCL / LCL available |
| Payment Terms | Support FOB \ CIF \ EXW quotations, and accept Letter of Credit (L/C). |
| Manufacturer | Greenrock Chemical(China Factory) |
Based on current marketvolatility and material availability.
17+ years in chemical exports.Fully compliant, reliable supply.Your B2B partner in bulk chemical procurement.
| Industry | Application | Process Description |
|---|---|---|
| Pharmaceutical R&D | Peptide synthesis reagent | Used as a chiral building block in coupling reactions during solid-phase peptide synthesis |
| Biochemistry | Protein structure studies | Applied to synthesize stereospecific peptides for investigating protein function |
| Organic synthesis | Chiral catalyst precursor | Employed in the synthesis of chiral auxiliaries or catalysts for asymmetric reactions |
| Analytical chemistry | Chiral separation standard | Used as a reference material in chiral chromatographic analysis |
| Materials science | Functional material synthesis | Applied in the preparation of organic functional materials with defined structures |
| Detection Item | Common Analytical Method | Method Overview |
|---|---|---|
| Assay (Purity) | HPLC-UV | Quantification by reverse-phase HPLC with UV detection at 268 nm using external standard calibration. |
| Chiral Purity | Chiral HPLC | Separation of D- and L-enantiomers on a chiral stationary phase; D-isomer peak area ratio calculated against total valine-related peaks. |
| Water Content | Karl Fischer Titration | Electrochemical titration with iodine reagent to determine water content based on stoichiometric reaction. |
| Residual Solvents | GC-FID | Headspace gas chromatography with flame ionization detection for quantification of common solvents (e.g., DMF, THF, ethyl acetate). |
| Heavy Metals | ICP-MS | Multi-element detection of toxic metals (Pb, Cd, Hg, As) after acid digestion using inductively coupled plasma mass spectrometry. |
| Residual Chloride | Ion Chromatography | Quantitative determination of chloride ions using suppressed conductivity detection after anion exchange separation. |
| Related Substances | HPLC-UV | Detection and quantification of structurally related impurities (e.g., Fmoc-Val-OH deprotection products, dipeptides) using gradient HPLC. |
| Optical Rotation | [alpha]D Measurement | Measurement of specific optical rotation at 589 nm using a polarimeter to confirm chiral integrity and identity. |
| pH (1% w/v aqueous suspension) | pH Meter | Direct measurement of pH in a defined aqueous suspension to assess acid-base character and residual reagents. |
| Loss on Drying | Gravimetric Analysis | Weight loss measured after drying under controlled temperature and vacuum to determine volatile content. |
| Melting Point | Capillary Melting Point Apparatus | Thermal transition observed as the temperature range at which solid-to-liquid phase change occurs. |
| Appearance | Visual Inspection | Assessment of physical form, color, and homogeneity against reference standard under controlled lighting conditions. |
| Test Item | Specification |
|---|---|
| Appearance | White solid |
| Purity | >=98.0% (LC-MS) |
| Water Content (KF) | <=0.5% |
| Total Impurities | <=2.0% |
| Single Impurity | <=0.5% |
| Optical Rotation | +15.0 to +19.0 deg (c=1, in DMF) |
| Melting Point | 128 to 132 °C |
| Identification (NMR) | Conforms to reference spectrum |
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| CAS/Product ID | *Required fields | |
| Lot/Batch Number | *Required fields | |
1. How do you ensure product quality consistency?
We rely on a mature China-based manufacturing system and implement strict batch control and quality inspection for every shipment. Our production process complies with ISO 9001 standards, and a COA is provided for each batch to ensure consistent and reliable quality.
2. Do you offer competitive pricing for bulk orders?
Yes, as a China-based manufacturer and bulk supplier, we provide tiered pricing based on order volume. We support FOB and CIF quotations, as well as L/C payment terms for large transactions to meet international trade requirements.
3. Can you support large-volume or long-term supply?
We have stable production capacity and a well-established supply chain, enabling continuous bulk supply. We support ton-level and container-level orders, as well as long-term cooperation projects.
4. What is your typical lead time?
For in-stock products, shipment can be arranged within 1–3 days. For bulk packaging or customized orders, lead time depends on the specific quantity and production schedule.
5. What documents do you provide?
We can provide complete documentation upon request, including COA, SDS, TDS, and other compliance certificates, meeting industrial procurement and export requirements.
6. Can you customize product specifications or packaging?
Yes, we support customization of parameters such as purity, impurities, residual solvents, and heavy metals. We also offer various bulk packaging options, including 25kg bags, drums, and IBC tanks, suitable for industrial applications and transportation.
7. What shipping options do you support?
We support both FCL (Full Container Load) and LCL (Less than Container Load) shipments, and can flexibly arrange logistics solutions based on order size to meet bulk chemical export needs.
8. Do you provide technical or application support?
Yes, we provide basic application guidance and technical support based on industry experience to help customers optimize product usage.
9. How do you handle compliance and export regulations?
We are familiar with international trade and export regulations, ensuring all products comply with relevant requirements. We also provide complete documentation to support smooth customs clearance and global delivery.